Bystrzejewski, M and Rummeli, M. H. and Gemming, T and Lange, H and Huczko, A (2010) Catalyst-free synthesis of onion-like carbon nanoparticles. New Carbon Materials, 25 (1). 1 - 8.
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Official URL: http://www.sciencedirect.com/science/article/B8H10...
Abstract
A one-step process for the synthesis of onion-like carbon nanoparticles is described. The process is based on a thermolysis of a NaN3-C6Cl6 mixture. The effect of buffer gas (Ar or air) on the yield, morphology, and structure of the carbon products was investigated by electron microscopy, X-ray diffraction, and Raman spectroscopy. The products contained carbon-onions, amorphous carbon nanoparticles, and NaCl. The byproducts were completely removed using a simple purification process. The formation of onion-like nanoparticles is likely caused by a shock wave, a rapid increase of pressure, during thermolysis, which induced the coalescence of phenyl radicals.
| Item Type: | Article |
|---|---|
| Uncontrolled Keywords: | Raman spectroscopy |
| Subjects: | Material Science > Nanofabrication processes and tools Material Science > Nanostructured materials |
| ID Code: | 8603 |
| Deposited By: | SPI |
| Deposited On: | 25 Mar 2010 21:50 |
| Last Modified: | 25 Mar 2010 21:50 |
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