Nano Archive

Synthesis and Characterization of CdS Microflowers

Amutha, Ramakrishnan and Akilandeswari, S. and Kannappan, A.N. and Muruganandham, Manickavachagam and Sillanpää, Mika (2010) Synthesis and Characterization of CdS Microflowers. Advanced Science Letters . ISSN 1936-6612

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Official URL: http://www.ingentaconnect.com/content/asp/asl/2010...

Abstract

In this manuscript, we have reported a template free fabrication of CdS microflowers by the thermal decomposition of cadmium thiocyanate complex at 300 C under open atmospheric condition. This synthetic methodology opens a new window for a well crystallized, single phase CdS preparation in large-scale. The formation of microflower morphology was investigated under various experimental conditions and the results imply that the decomposition temperature, co-solvents, cadmium and sulfur precursors played an important role on the formation of microflower morphology. The synthesized CdS has been characterized by using XRD, XPS, FE-SEM and HR-TEM. The XRD patterns revealed that the formation of pure wurtzite phase at all decomposition temperature and the XPS results also confirmed the formation of CdS. The FE-SEM picture indicated that the microflower morphology was self-assembled by the intact of thin nano-sheets. A plausible mechanism of CdS microflower formation has been discussed on the basis of the experimental results.

Item Type:Article
Subjects:Material Science > Nanochemistry
Material Science > Nanostructured materials
ID Code:11721
Deposited By:Prof. Mika Sillanpää
Deposited On:13 Jan 2012 12:53
Last Modified:13 Jan 2012 12:53

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